有機(jī)化合物結(jié)構(gòu)鑒定

內(nèi)容概要

　　第4版新增了20%實(shí)驗(yàn)數(shù)據(jù)，增添了19F和31P
NMR兩個(gè)章節(jié)，以及一些重要的Raman光譜。本書以獨(dú)特的表示方式—通過文字、表格、圖表、圖形—將核心的參考數(shù)據(jù)以簡(jiǎn)潔的編匯形式予以呈現(xiàn)，通過實(shí)踐指導(dǎo)詮釋了包括NMR,
IR, UV/Vis和質(zhì)譜數(shù)據(jù)以及相對(duì)應(yīng)各自的化合物的結(jié)構(gòu)特征。除了光譜使用的常規(guī)溶劑，還包含了標(biāo)準(zhǔn)試劑、MALDI 和 FAB
MS基質(zhì)材料、質(zhì)譜碎片峰的基本規(guī)律以及代表性化合物的UV/Vis光譜。本書不僅適用于學(xué)生課程學(xué)習(xí)和練習(xí)，而且高級(jí)學(xué)習(xí)者可借此書擴(kuò)展閱讀。同時(shí)具有初級(jí)光譜知識(shí)的技術(shù)人員可以使用此書，專業(yè)人士還可以使用書中的參考數(shù)據(jù)處理日常光譜信息解析。

作者簡(jiǎn)介

作者：(瑞士)普雷奇(Erno Pretsch) 等

書籍目錄

1 Introduction
1.1 Scope and Organization
1.2 Abbreviations and Symbols
2 Summary Tables
2.1 General Tables
2.1.1 Calculation of the Number of Double Bond Equivalents from the
Molecular Formula
2.1.2 Properties of Selected Nuclei
2.2 BC NMR Spectroscopy
2.3 IH NMR Spectroscopy
2.4 IR Spectroscopy
2.5 Mass Spectrometry
2 5.1 Average Masses of Naturally Occurring Elements with Masses
and Representative Relative Abundances of lsotopes
2.5.2 Ranges of Naturall sotope Abundances of Selected
Elements
2.5.3 Isotope Patterns ofNaturally Occurring Elements
2.5.4 Calculationoflsotope Distributions
2.5.5 Isotopic Abundances of Various Combinations of Chlorine,
Bromine,Sulfur,and Silicon
2.5.6 Isotope Pattems of Combinations of Cland Br
2.5.7 Indicators of the Presence of Heteroatoms
2.5.8 Rules for Determining the Relative Molecular Weight
(Mr)
2.5.9 Homologous Mass Series aslndications of StructuralType
2.5.10 Mass Correlation Table
2.5.11 References
2.6 UV/Vis Spectroscopy
3 Combination Tables
3.1 Alkanes,Cycloalkanes N
3.2 Alkenes,Cycloalkenes N
33 Alkynes
3.4 Aromatic Hydrocarbons
3.5 Heteroaromatic Compounds
3.6 Halogen Compounds
3.7 Oxygen Compounds
3.7.1 Alcohol; and Phenols
3.7.2 Ethers
3.8 Nitrogen Compounds
3.8.1 Amines
3.8.2 Nitro Compounds
3.9 Thiols and Sulfides
3.10 Carbonyl Compounds
3.10.1 Aldehydes
3.10.2 Ketones
3.10.3 CarboxylicAcids
3.10.4 Esters and Lactones
3.10.5 Amides and Lactams
4 13C NMR Spectroscopy
4.1 Alkanes
4.1.1 Chemical Shifts
4.1.2 Coupling Constants
4.1.3 References
4.2 Alkenes
4.2.1 Chemical Shifts
4.2.2 Coupling Constants
4.2.3 References
4.3 Alkynes
4.3.1 Chemical Shifts
4.3.2 Coupling Constants
4.3.3 References
4.4 Alicyclics
4.4.1 Chemical Shifts
4.4.2 Coupling Constants
4.5 Aromatic Hydrocarbons
4.5.1 Chemical Shifts
4.5.2 Coupling Constants
4.5.3 References
4.6 Heteroaromatic Compounds
4.6.1 Chemical Shifts
4.6.2 Coupling Constants
4.7 Halogen Compounds
4.7.1 Fluoro Compounds
4.7.2 Chloro Compounds
4.7.3 Bromo Compounds
4.7.4 Iodo Compounds
4.7.5 References
4.8 Alcohols,Ethers,and Related Compounds
4.8.1 Alcohols
4.8.2 Ethers
4.9 Nitrogen Compounds
4.9.1 Amines
4.9.2 Nitro and Nitroso Compounds
4.9.3 Nitrosamines and Nitramines
4.9.4 Azo and Azoxy Compounds
4.9.5 Imines and Oximes
4.9.6 Hydrazones and Carbodiimides
4.9.7 Nitriles and lsonitriles
4.9.8 Isocyanates,Thiocyanates,andlso thiocyanates
4.10 SulfurCompounds
4.10.1 Tluols
4.10.2 Sulfides
4.10.3 Disulfides and Sulfonium Salts
4.10.4 Sulfoxides and Sulfones
4.10.5 Sulfonic and Sulfinic Acids and Derivatives
4.10.6 Sulfurous and Sulfuric Acid Derivatives
4.10.7 Sulfur-Containing CarbonylDerivatives
4.11 CarbonyICompounds
4.11.1 Aldehydes
4.11.2 Ketones
4.11.3 CarboxylicAcids
4.11.4 Esters and Lactones
4.11.5 Amides and Lactams
4.11.6 Miscellaneous Carbonyl Derivatives
4.12 Miscellaneous Compounds
4.12.1 Compounds with GroupIV Elements
4.12.2 Phosphorus Compounds
4.12.3 Miscellaneous Organometallic Compounds
……
5 H NMR Spectroscopy
6 Heteronuclear NMR Spectroscopy
7 IR Spectroscopy
8 Mass Spectrometry
9 UV/Vis Spectroscopy
Subject Index

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